Hi Richard, Our powder diffraction station, SSRL Beam Line 2-1, has the highest angular resolution of our 3 diffractometer beam lines, but it has only a 2-circle diffractometer. You experiment sounds straight forward, but likely requires a 4-circle. I have a diffraction beam line meeting with staff scientist today and will bring up your experiment. I will get back to you with a recommendation by tomorrow. Regards, Bart